Photochemisch orthogonale Festphasensynthesen
eBook - PDF

Photochemisch orthogonale Festphasensynthesen

,
  1. 318 pages
  2. English
  3. PDF
  4. Available on iOS & Android
eBook - PDF

Photochemisch orthogonale Festphasensynthesen

,

About this book

Schutzgruppenstrategien, in denen Licht als "Abspaltungsreagens" eingesetzt werden kann, sind eine interessante Erweiterung des chemischen Methodenarsenals, da unter milden, substratschonenden Bedingungen und ohne Kontamination der Substrate mit Reagentien gearbeitet werden kann.Es wurde eine photochemisch orthogonale Schutzgruppenstrategie fĂŒr die Festphasen-Peptidsynthese entwickelt. Die Kombination von Pivaloyllinkern- und NVOC-Schutzgruppen wurde zu diesem Zweck eingehend untersucht. Die photochemisch orthogonale Methode erlaubte die wellenlĂ€ngenselektive Anregung verschiedener photolabiler Schutzgruppen und lieferte die Zielverbindungen ohne weitere Aufarbeitung in hoher Reinheit.Die Brauchbarkeit des photolabilen Pivaloyllinkers zur Synthese grĂ¶ĂŸerer caged-Peptide (7 - 15AminosĂ€uren) nach konventionellen Peptidsyntheseprotokollen und anschließenderphotolytischer Freisetzung (uncaging) der C-terminal gebundenen Peptide unter in-vivo-Bedingungen wurde untersucht.

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Information

Publisher
Cuvillier Verlag
Year
2008
Print ISBN
9783867276443
eBook ISBN
9783736926448
Edition
1

Table of contents

  1. 9783867276443.jpg
  2. Diss1-klein.pdf