Microwave-assisted synthesis has gained much attention in recent years. The applications of microwave irradiation are used for carrying out chemical transformations, which are pollution free, eco-friendly, low cost and offer high yields together with simplicity in processing and handling. The salient features of microwave approach are shorter reaction times, simple reaction conditions and enhancements in yields.In 21st century the main objective is to develop environmental friendly and pollution free techniques; microwave synthesis fit into this profile. So many advantages and superiority over conventional methods make these techniques to prominent tools of green technology. In the present research studies, our efforts are synthesized of some newly compounds from the conventional as well as microwave methods. These synthesized compounds characterized by various physicochemical and spectral analyses.