For one thing, the book presents research aimed at obtaining thin phosphate layers that offer good corrosion protection of finished parts. The other aim was to develop techniques that result in coatings with good lubricating properties, as they are required in plastic deformation processing. Keywords: Thin Films Deposition, Phosphate Coatings, Surface-Active Agents, Zinc Phosphates, Degreasing, Lubricating Films, Corrosion Protective Films, Anticorrosive Phosphate Films, Phosphating Techniques, Plastic Deformation Processing, Phosphating of Iron-Based Metallic Parts, Thin Film Characterization, Optical Microscopy, Electronic Microscopy, EDX Analysis, XRD Analysis, Optical Profilometry, Corrosion Tests, FTIR Spectroscopy, Tribological Tests, SEM-EDX Analysis.

- 158 pages
- English
- PDF
- Available on iOS & Android
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Table of contents
- Table of Contents
- Introduction
- Chapter 1
- Known Phosphating Technologies
- 1.1 Specific Phosphating Processes
- 1.2 Classical Phosphating Solutions
- 1.3 Modern Phosphating Procedures
- 1.4 Study of the Morphology and Structure of Thin Films depending on the Production Process
- Chapter 2
- Creation of Thin Phosphate Films in the Laboratory
- 2.1 Experimental Protocol Development
- 2.2 Support Material Used for the Research (Blanks)
- 2.3 Experimental Equipment
- 2.4 Solution Preparation
- 2.5 Modeling of the Structure of the Phosphate Coating from the Viewpoint of the Surface Processes
- Chapter 3
- Modern Procedures for the Creation of Thin Anticorrosive Lubricating Phosphate Films by Addition and Subtraction
- 3.1 New Phosphating Procedures by Conversion as Thin Surface Films
- 3.2 Development of the Technological Flow Applying to Microcrystalline Phosphating of Iron-Based Metallic Parts Involving the Additive/Subtracting System
- 3.3 Crystalline Lubricant Phosphating of Iron-Based Metallic Parts Involving the Subtractive/Additive System
- 3.4 Development of the Technological Flow of Crystalline Lubricant Phosphating of Iron-Based Metallic Parts in the Subtractive/Additive System
- 3.5 Chemical Composition and Work System Parameters Applying to Crystalline Chemical Phosphating in the Additive/Subtractive System
- 3.6 Chemical Composition and Work System Parameters Applying to Crystalline Chemical Phosphating in the Subtractive/Additive System
- 3.7 Designing Laboratory Equipment for Crystalline Chemical Phosphating in the Additive/Subtractive and Subtractive/Additive Systems
- Chapter 4
- Thin Phosphate Film Characterization Methods and Techniques
- 4.1 Introduction
- 4.2 Optical Microscopy
- 4.3 Electronic Microscopy
- 4.4 EDX Analysis
- 4.5 XRD Analysis
- 4.6 Optic Profilometry
- 4.7 Corrosion Tests
- 4.8 FTIR Spectroscopy
- 4.9 Tribological Tests
- 4.10 Determination of the Drawing Force
- Chapter 5
- Characterization of Thin Phosphate Films
- 5.1 Indexing of Specimens Used in our Research
- 5.2 Optical Microscopy (OM) Studies
- 5.3 SEM-EDX Analysis
- 5.4 XRD Diffractometric Analysis
- 5.5 MicroFTIR Spectroscopy Analysis
- 5.6 Study of Resistance to Corrosion in NaCl 0.1M Solution
- 5.7 3D Profilometric Analysis
- 5.8. Tribological Tests
- 5.9 Analysis of Operating Behavior of the Phosphate Films
- References
- Keyword Index
- About the Authors
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