Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

John S. Harwood, Huaping Mo

• Publisher: Academic Press
• Year: 2015
• Print ISBN:
  9780128006894
• eBook ISBN:
  9780128007198
• Topic: Physical Sciences
• Subtopic: Electromagnetism

Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge's High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). - Written by experts in solution-state NMR spectroscopy - Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer - Includes detailed appendices and sample questions for lab reports

Table of contents

• Cover image
• Title page
• Table of Contents
• Copyright
• Acknowledgments
• Introduction
• Chapter 1. Basics and Spectrometer Performance Checks
• Chapter 2. Multiple Irradiation and Multiple Pulse Experiments
• Chapter 3. Polarization Transfer and Its Applications
• Chapter 4. Homonuclear Correlation Experiments
• Chapter 5. PFG (Pulsed Field Gradient) Experiments
• Chapter 6. Introduction to NMR of Biomolecules in H2O
• Chapter 7. Selective Experiments Using Shaped Pulses
• Chapter 8. Diffusion Measurements and DOSY (Diffusion Ordered SpectroscopY)